pe
pep-10953 v1 CC-BY-SA-4.0

Pal-AHK: copper-binding peptide studied for hair and skin

A lab-made cosmetic ingredient that may help boost collagen and support hair follicles; used in skincare, not an approved drug.

statusdesigned target? length3 aa refs1
snapshot in_vitro 0% confidence
Class
Cosmeceutical lipopeptide (palmitoylated copper-binding tripeptide)
Status
Cosmetic ingredient; not approved as a drug in any jurisdiction
Best-supported effect
Dermal papilla cell anti-apoptotic signaling and hair follicle elongation in cell culture and ex vivo assay systems (AHK-Cu form only)
Main caveat
All biological activity evidence is in vitro and ex vivo only, using the copper-complexed form (AHK-Cu) — not the palmitoylated commercial form (Pal-AHK); no animal in vivo or human trial data exist
status 1 / 5
sequence3 aa
13
AHK
overview readme

Snapshot

Class: Cosmeceutical lipopeptide (palmitoylated copper-binding tripeptide)
Evidence tier: In vitro / assay evidence
Status: Cosmetic ingredient; not approved as a drug in any jurisdiction
Best-supported effect: Dermal papilla cell anti-apoptotic signaling and hair follicle elongation in cell culture and ex vivo assay systems (AHK-Cu form)
Main caveat: All biological activity evidence is in vitro and ex vivo only, using the copper-complexed form (AHK-Cu) — not the palmitoylated commercial form (Pal-AHK); no animal in vivo or human trial data exist


What this is

Pal-AHK (Palmitoyl Tripeptide-28, also referenced under the older designation Palmitoyl Tripeptide-3) is a synthetic lipopeptide consisting of the tripeptide alanine-histidine-lysine (AHK) conjugated to palmitic acid at the N-terminus. The palmitoyl modification increases lipophilicity, which is intended to improve penetration through the stratum corneum in topical cosmeceutical formulations. The AHK tripeptide belongs to the copper-binding tripeptide family and forms the AHK-Cu complex (Copper Tripeptide-3) in the presence of copper ions; the copper-complexed form is the active species in all published in vitro research. Pal-AHK is structurally related to Pal-GHK (Palmitoyl Tripeptide-1), differing at the first amino acid (alanine versus glycine), but has a distinct and far thinner research profile centered on hair follicle and dermal papilla biology rather than the matrikine-driven collagen signaling associated with GHK. It is marketed as a cosmeceutical ingredient for hair growth and skin anti-aging; these commercial uses rest on a narrow preclinical evidence base.


Evidence map

Evidence layerGradeWhat it supports
HumanNoneNo published human clinical trials for Pal-AHK or AHK-Cu for any endpoint
AnimalNoneNo published in vivo animal hair-growth or skin studies for AHK-family peptides
In vitro / ex vivoWeak — single study, copper-complexed form onlyHair follicle elongation ex vivo; dermal papilla cell anti-apoptotic signaling; fibroblast collagen and VEGF responses in cell culture
ComputationalNoneNo docking or structure-prediction data identified
MechanismPlausibleAnti-apoptotic Bcl-2/Bax modulation, VEGF upregulation, TGF-β1 suppression, and collagen type I stimulation are mechanistically described from the in vitro data; pathway from palmitoylated form to AHK-Cu activity is assumed, not demonstrated

The in vitro and ex vivo evidence derives almost entirely from a single publication (Pyo et al., 2007); independent peer-reviewed replication is absent. Whether the palmitoylated commercial form (Pal-AHK) is equivalent to the copper-complexed research form (AHK-Cu) at the cellular level has not been characterized.


Claim check

ClaimVerdictEvidence layerConfidence
Hair follicle elongation and dermal papilla cell survival (ex vivo / in vitro, copper-complexed form)Supported (in vitro / ex vivo)In vitroLow — single study, AHK-Cu form, not Pal-AHK; no independent replication
Collagen type I synthesis stimulation in fibroblast culturesSupported (in vitro)In vitroLow — single study; no independent replication
Hair growth stimulation in living humansNot establishedNoneHigh
Pal-AHK is equivalent to AHK-Cu in biological activityNot establishedNoneHigh — assumed by commercial use but not characterized
Skin pigmentation and tone improvementNot establishedNoneHigh — no peer-reviewed mechanistic data; commercially driven claim
Safe and effective for injectable useNot establishedNoneHigh — cosmetic preparations are not sterile injectable products; no clinical or efficacy data exist for this route

Assay conditions

This section reports concentrations and conditions used in the published in vitro and ex vivo assays. It does not establish topical cosmeceutical dose, frequency, or any human exposure.

ContextSystemAssay conditionTimepointEndpointLimitation
In vitro — dermal papilla cell proliferationHuman dermal papilla cells (cultured)AHK-Cu at 10⁻¹² to 10⁻⁹ MNot individually extractedDPC proliferation; Bcl-2/Bax ratio; cleaved caspase-3 and PARP levelsAHK-Cu form only; not Pal-AHK; single study; concentration-to-topical-product translation not established
Ex vivo — hair follicle elongationCultured human hair folliclesAHK-Cu at picomolar to nanomolar concentrationsNot individually extractedFollicle elongationEx vivo organ culture, not in vivo; AHK-Cu form only; no independent replication
In vitro — fibroblast collagen and VEGFHuman dermal fibroblast culturesAHK-Cu (concentration not separately extracted)Not individually extractedCollagen type I (up to 300% increase reported); VEGF secretion; TGF-β1 secretionSingle study; cell culture system; AHK-Cu form; translation to topical application not established

Assay limitations

  • All published biological activity data use the copper-complexed form (AHK-Cu, Copper Tripeptide-3), not the palmitoylated commercial form (Pal-AHK, Palmitoyl Tripeptide-28). Whether Pal-AHK is cleaved to release free AHK intracellularly, or whether the intact palmitoylated molecule acts equivalently to AHK-Cu at the cell surface, has not been characterized.
  • The entire hair-growth signal traces to a single publication (Pyo et al., 2007); independent peer-reviewed replication of the core findings does not appear in the available literature.
  • Ex vivo hair follicle culture and in vitro DPC assays do not establish whether follicle-level effects translate to in vivo hair growth in intact skin or in human scalp.
  • In vitro concentration ranges (picomolar to nanomolar for AHK-Cu) do not translate directly to topical product percentage concentrations; actual delivery of active peptide to dermal papilla cells from commercial topical formulations is not quantified.
  • No formal cell-viability or cytotoxicity data beyond the proliferation endpoints are reported in available literature.
  • No animal or human safety or efficacy data are identified.

Mechanism

The AHK tripeptide, in its copper-complexed form (AHK-Cu), exerts biological effects through anti-apoptotic signaling in dermal papilla cells (DPCs) and fibroblast stimulation. In dermal papilla cells, AHK-Cu elevates the Bcl-2/Bax ratio by upregulating the anti-apoptotic protein Bcl-2 and downregulating the pro-apoptotic protein Bax; it also reduces cleaved caspase-3 (by approximately 42.7% at 10⁻⁹ M) and cleaved PARP (by approximately 77.5%), indicating reduced programmed cell death. In dermal fibroblasts, AHK-Cu stimulates proliferation, elevates VEGF secretion (supporting angiogenesis and follicular vascularization), and decreases TGF-β1 secretion — TGF-β1 being a catagen-inducing factor that suppresses hair follicle cycling into the growth phase. Collagen type I production in fibroblast cultures was reported to increase substantially. The copper-coordination capacity of the AHK sequence resides in the histidine imidazole ring and the lysine amine group. The palmitoyl modification (C16 fatty acid at the N-terminus) is intended to enhance partitioning into the lipid-rich stratum corneum; whether Pal-AHK is subsequently cleaved to release biologically active AHK or copper complex intracellularly, or acts as an intact molecule at the receptor/cell surface, is uncharacterized. No receptor-level binding data exist. The mechanistic basis for marketed pigmentation claims is absent from published literature.


Chemistry

FieldValue
Full namePalmitoyl-Ala-His-Lys; Palmitoyl Tripeptide-28
Older INCI designationPalmitoyl Tripeptide-3
Amino-acid chainAla-His-Lys (three residues)
Length3 amino acids
TopologyLinear
ModificationN-terminal palmitoyl group (C16 fatty acid, palmitic acid conjugation)
Copper-complexed formAHK-Cu (Copper Tripeptide-3); active form used in published assay research
Molecular formulaC₃₁H₅₆N₆O₅
Molecular weight~592.8 Da
Sequence confidenceVerified (source-consistent)

Regulatory status

Region / bodyStatusNotes
USCosmetic ingredient; not a drugRegulated under FDA cosmetic law; over-the-counter sale in finished cosmetic formulations is permitted; not approved as a drug for hair loss, skin aging, or any medical indication; hair-loss drug claims are not permitted on cosmetic labels
EUPermitted cosmetic ingredientListed in the CosIng database; safety reviews of related copper tripeptides and palmitoyl tripeptides have not raised concerns at typical formulation levels (per available sources)
UK, Canada, Australia, JapanPermitted as cosmetic ingredientPer available sources, broad international cosmetic market access; status not independently refreshed in this card
WADANot listed as prohibitedTopical cosmeceutical use; negligible systemic exposure relevant to performance (per available sources; current list status not independently verified in this card)

No approved therapeutic status exists for Pal-AHK in any attached source. This card describes a cosmetic ingredient, not an approved medicine.


Open questions

  • Human translation: No controlled human trials for Pal-AHK or AHK-Cu exist for hair growth, skin anti-aging, or any other endpoint. Whether the in vitro and ex vivo signals observed with AHK-Cu translate to detectable clinical benefit in humans is unknown.
  • Pal-AHK vs. AHK-Cu equivalence: Whether the palmitoylated form is cleaved or otherwise converted to an active copper complex in vivo, or whether it reaches dermal papilla cells with retained bioactivity, has not been characterized. All published efficacy data use AHK-Cu, not Pal-AHK.
  • Independent replication: The foundational hair-growth findings (Pyo et al., 2007) have not been independently replicated in peer-reviewed literature. The entire biological plausibility claim rests on a single research group's work.
  • In vivo animal hair-growth models: No published rodent or other in vivo models have been conducted for AHK-family peptides, representing a notable gap between ex vivo organ culture and any in vivo system.
  • Skin penetration and delivery quantification: Whether topical cosmeceutical formulations deliver biologically relevant concentrations of Pal-AHK or AHK to dermal papilla cells or fibroblasts in intact human skin is not established.
  • Pigmentation mechanism: No peer-reviewed data demonstrate any effect of Pal-AHK or AHK-Cu on melanogenesis or melanocyte biology. The marketed pigmentation claim lacks published mechanistic basis.
  • Long-term safety: Chronic topical safety under sustained use — particularly for scalp formulations — has not been formally evaluated. The long-term biology of topical copper tripeptide exposure, including cumulative copper coordination effects, is not characterized.
Hypotheses4 directions▾ collapse

Research directions for this peptide, selected from the current sources — hypotheses you can explore and model. None of it is proven yet; tap any one to see the full thinking.

openupdated 2026-06-05

Does attaching a fatty acid to AHK's active end, as done in the commercial product, permanently block the part of the molecule that must grab copper to function?

If the commercial formulation is inadvertently self-sabotaging, reformulating with the copper-binding end of AHK left free could dramatically improve efficacy for people using the product for hair thinning or skin care. It would also reveal that decades of cosmetic industry investment in this particular lipopeptide form may need to be redirected.

The hypothesis
Pal-AHK (the palmitoylated commercial form) is biologically inactive as delivered in topical formulations because the palmitoyl group at the N-terminus permanently blocks the free amine required for ATCUN copper coordination, and the anti-apoptotic activity attributed to the ingredient in cell-culture studies actually reflects activity of residual unpalmitoylated AHK-Cu contaminating the synthesis batch.
Why it’s plausible
The ATCUN motif requires a free primary amine at the N-terminus for Cu(II) coordination. Palmitoylation at the N-terminal amine converts it to an amide, abolishing the primary amine. Without the free N-terminal amine, the His imidazole alone cannot form the stable tridentate Cu(II) chelate that defines ATCUN activity. If Pal-AHK cannot bind copper, it cannot form AHK-Cu, and all biological activity attributed to AHK-Cu would be absent. The readme explicitly notes that all biological evidence uses AHK-Cu, not Pal-AHK, which is consistent with this concern. The commercial ingredient may rely on residual deprotected peptide or in situ hydrolysis of the palmitoyl amide under skin conditions.
Why it matters
If Pal-AHK cannot form the active copper complex because palmitoylation blocks the ATCUN amine, then the entire commercial rationale for the ingredient is flawed. This would imply that a formulation providing AHK peptide without N-palmitoylation (e.g., C-terminal palmitoylation or a different lipid attachment point) would be dramatically more effective, representing a major reformulation opportunity.
Plausibility.75
Novelty.70
Impact.80
Basis · grounding3 computed/notes
[1]
noteExplicit statement that all biological activity data uses the copper-complexed form (AHK-Cu), not the palmitoylated commercial form (Pal-AHK); this inconsistency is flagged as the main caveat.
[2]
sequenceAHK: the N-terminal amine (on Ala) is the first coordination atom of the ATCUN motif. Palmitoylation replaces this NH2 with an amide N, which is a far weaker Cu(II) ligand with pKa too low for stable coordination under physiological pH.
[3]
sourceStructural integrity of peptide modifications and their effect on bioactivity are discussed; N-terminal modification is among the most consequential for activity, consistent with the concern raised.
openupdated 2026-06-05

Does AHK-Cu work by catalytically dismantling the reactive oxygen species that accumulate in hair follicle cells under stress, similar to how the body's own superoxide dismutase enzyme works?

If AHK-Cu is a catalytic antioxidant, it could protect hair follicles at very low doses, making it more feasible to deliver enough of it through the skin to actually work. This would be relevant to anyone experiencing hair thinning linked to oxidative stress, including androgenic alopecia, which affects roughly half of all adults over 50.

The hypothesis
AHK-Cu promotes dermal papilla cell survival under oxidative stress by acting as a superoxide dismutase (SOD) mimetic, using its histidine-copper coordination complex to catalytically disproportionate superoxide radicals, thereby reducing mitochondrial ROS accumulation that drives the pro-apoptotic signaling cascade in androgen-stressed hair follicles.
Why it’s plausible
The AHK (Ala-His-Lys) tripeptide in its copper-complexed form (AHK-Cu) coordinates Cu(II) through the histidine imidazole and the N-terminal amine in a geometry closely resembling the active site of Cu/Zn-SOD and the ATCUN (amino terminal copper and nickel binding) motif. ATCUN-Cu complexes have documented SOD-mimetic activity. Dermal papilla cells under androgenic stress generate elevated mitochondrial superoxide, which drives apoptosis. AHK-Cu's SOD-mimetic activity would provide a catalytic rather than stoichiometric antioxidant defense, explaining why low concentrations of the copper complex show anti-apoptotic effects in cell culture. This mechanism is distinct from the matrikine growth factor signaling proposed for GHK-Cu.
Why it matters
If AHK-Cu is a catalytic ROS scavenger at the ATCUN level, it would be active at sub-micromolar concentrations (catalytic turnover) rather than requiring stoichiometric doses. This would resolve the key translation challenge for topical copper peptides: penetrating the dermis at high enough concentrations to exert biological effects at stoichiometric doses has always been doubted, but catalytic activity at low concentrations is far more achievable.
Plausibility.65
Novelty.60
Impact.70
Basis · grounding3 computed/notes
[1]
noteAHK-Cu (the copper-complexed form) is identified as the biologically active species; anti-apoptotic activity in dermal papilla cell cultures is the best-supported effect.
[2]
sequenceAHK: Ala-His-Lys. The amino-terminal amine plus imidazole of His at position 2 forms the canonical ATCUN Cu(II) chelation motif (NH2-aa1-His); Lys at position 3 adds a second amine that can further stabilize the complex.
[3]
sourceCopper coordination and catalytic effects on biomolecular processes are discussed in the membrane context, consistent with the mechanistic relevance of copper complexation in biological settings.
openupdated 2026-06-05

Does the methyl group on alanine in AHK-Cu change the shape of the copper coordination complex enough to switch it from collagen-stimulating (GHK-Cu) to hair-follicle-protecting activity?

Understanding why such a tiny chemical difference between two very similar peptides produces such different results would give scientists a precise design rule for engineering copper peptides with specific skin or hair benefits on demand, potentially replacing years of empirical screening with rational design.

The hypothesis
Substituting alanine at position 1 of AHK with glycine (producing GHK) fundamentally alters the copper coordination geometry by removing the methyl side chain that restricts Cu(II) from adopting an additional axial coordination position, and this geometric difference explains why GHK-Cu has a distinct and broader biological activity profile (matrikine collagen signaling) compared to AHK-Cu (anti-apoptotic/hair follicle).
Why it’s plausible
GHK-Cu (Gly-His-Lys-Cu) is structurally related to AHK-Cu (Ala-His-Lys-Cu) with only the first position differing (Gly vs. Ala). Glycine has no side chain, allowing the Cu(II) center to adopt a planar or weakly axially coordinated geometry. Alanine's methyl group introduces steric hindrance at the coordination sphere, favoring a distorted square planar or 5-coordinate geometry for the Cu(II). These geometrically distinct copper complexes would have different redox potentials and different protein surface interaction profiles, leading to activation of different downstream signaling pathways (matrikine TGF-beta signaling for GHK-Cu vs. anti-apoptotic Bcl-2 pathway for AHK-Cu). This is directly testable by comparing the two copper complexes side by side on identical cell types.
Why it matters
If a single methyl group difference between Gly and Ala determines the entire biological pathway activated by the copper complex, it reveals copper coordination geometry as the primary pharmacophoric determinant for this class of peptides. This would guide the systematic design of copper tripeptides with pre-specified biological activities by controlling the first-position side chain.
Plausibility.60
Novelty.60
Impact.60
Basis · grounding3 computed/notes
[1]
noteAHK-Cu (hair follicle anti-apoptotic) and Pal-GHK (matrikine collagen signaling) are stated to have distinct biological activities despite differing by only the first amino acid, this divergence requires a mechanistic explanation.
[2]
sequenceAHK: Ala at position 1 provides a methyl side chain adjacent to the ATCUN N-terminal amine copper coordination; versus GHK: Gly at position 1 has no side chain. The steric difference is minimal in peptide terms but geometrically significant for transition metal coordination.
[3]
sourceReceptor tyrosine kinase signaling divergence based on ligand structural variation is noted, supporting the concept that small structural changes can determine pathway selectivity in receptor/enzyme-ligand systems.
openupdated 2026-06-05

Could conjugating AHK to a fragment of hyaluronic acid direct the peptide specifically to the hair follicle cells that express the hyaluronic acid receptor, delivering a therapeutic dose where it is actually needed?

One of the biggest obstacles to turning AHK-Cu from a laboratory finding into a real hair-loss treatment is getting enough of it into the right place under the skin. A targeted delivery system that homes in on hair follicle cells could bridge that gap, potentially making an effective topical treatment for common hair thinning available without injections.

The hypothesis
Conjugating AHK to a hyaluronic acid (HA) oligosaccharide via its lysine side chain amine would create a follicle-targeting copper-peptide construct that exploits CD44 receptor expression on dermal papilla cells to concentrate AHK-Cu specifically at the target cells, increasing local copper-peptide concentration 10-100 fold over passive diffusion from a topical product.
Why it’s plausible
Dermal papilla cells express CD44, the hyaluronic acid receptor, at high levels. HA oligosaccharides (4-8 disaccharide units) bind CD44 with low micromolar affinity and are internalized by receptor-mediated endocytosis. Conjugating AHK via its lysine side-chain epsilon-amine (leaving the N-terminal amine free for copper coordination) to an HA oligosaccharide would create a bivalent construct with HA providing dermal papilla targeting and AHK-Cu providing the anti-apoptotic copper complex payload. The lysine side chain amine is not part of the ATCUN motif, so its modification would not abolish copper binding. This is an addressable engineering challenge given available HA-conjugation chemistry.
Why it matters
The fundamental barrier to AHK-Cu efficacy in vivo is achieving sufficient local concentration at dermal papilla cells through skin. A CD44-targeted delivery system would solve this without requiring systemic administration, making a topical hair-loss treatment genuinely viable rather than speculative.
Plausibility.60
Novelty.50
Impact.60
Basis · grounding3 computed/notes
[1]
noteAll efficacy data is in vitro and ex vivo, the primary unresolved question is whether sufficient concentrations can be achieved at dermal papilla cells in vivo; targeted delivery would directly address this.
[2]
sequenceAHK: Lys at position 3 provides an epsilon-amine available for conjugation chemistry (NHS ester, reductive amination) while N-terminal Ala amine remains free for ATCUN copper coordination.
[3]
sourceAlternative delivery strategies including targeted formulation approaches for peptides are discussed as solutions to stability and tissue-targeting challenges, HA-CD44 targeting is consistent with this design space.
details expand to inspect
3-letter notation
Ala-His-Lys
citationbibtex
peptidemodel (2026). Pal-AHK: copper-binding peptide studied for hair and skin (pep-10953, v1). PeptideModel. https://peptidemodel.com/card/pep-10953
@peptide{pep10953,
  sequence = {AHK},
  target   = {},
  author   = {peptidemodel},
  year     = {2026},
  status   = {designed}
}
clinical trials 0 trials · checked 2026-05-09
0
no registered clinical trials as of 2026-05-09; we'll re-check periodically
references 1 papers
[1]
A yeast toxic mutant of HET-s amyloid disrupts membrane integrity
Ta, Ha Phuong et al. Biochimica et Biophysica Acta (BBA) - Biomembranes 2012
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